N-(2,4,6-Trimethyl­phen­yl)formamide

نویسندگان

  • Marilé Landman
  • Belinda van der Westhuizen
  • Daniela I. Bezuidenhout
  • David C. Liles
چکیده

The title compound, C(10)H(13)NO, was obtained as the unexpected, almost exclusive, product in the attempted synthesis of a manganese(I)-N-heterocyclic carbene (NHC) complex. The dihedral angle between the planes of the formamide moiety and the aryl ring is 68.06 (10)°. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds, forming infinite chains along the c axis.

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منابع مشابه

(2,4,6-Trimethyl­phen­yl){2-[N-(2,4,6-trimethyl­phen­yl)formamido]­eth­yl}ammonium chloride

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1-(3-Ammonio­methyl-2,4,6-trimethyl­benz­yl)-3-(2,4,6-trimethyl­phen­yl)imidazol-1-ium dibromide monohydrate

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N-(2,4,6-Trimethyl­phen­yl)succinamic acid

The amide bond in the title compound {systematic name: 3-[(2,4,6-trimethyl-phen-yl)amino-carbon-yl]propionic acid}, C(13)H(17)NO(3), has a trans conformation. In the crystal, two mol-ecules form a centrosymmetric dimer connected by pairs of O-H⋯O hydrogen bonds. Inter-molecular N-H⋯O hydrogen bonds link the dimers into a three dimensional network.

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Dibromidobis[1-(2,4,6-trimethyl­phen­yl)-1,4,5,6-tetra­hydro­pyrimidine-κN 3]palladium(II)

In the title complex, [PdBr(2)(C(13)H(18)N(2))(2)], the Pd(II) atom is situated on an inversion center. The tetra-hydro-pyrimidine group of the N-(2,4,6-trimethyl-phen-yl)-1,4,5,6-tetra-hydro-pyrimidine ligand is twisted from the square (PdN(2)Br(2)) coordination plane with a C-N-Pd-Br torsion angle of 81.8 (4)°; this is different from the angle of 43.47 (14)°, reported in a closely related str...

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عنوان ژورنال:

دوره 67  شماره 

صفحات  -

تاریخ انتشار 2010